- Safety goggles
- Laboratory gloves
- Measuring cylinder (10 mL)
- Transfer pipet
- Volumetric flask (1 L)
- Distilled water
- Concentrated HCl (12 M)
- Dropper
Procedure:
Step 1: Calculate the Volume Required
The formula to calculate the volume of a concentrated solution required is:
*Volume of concentrated solution = Molarity of desired solution * Volume of desired solution / Molarity of concentrated solution*
In this case, we have:
- Molarity of desired solution (HCl) = 0.05 N
- Volume of desired solution = 1 L
- Molarity of concentrated HCl = 12 M
Substituting these values into the formula, we get:
Volume of concentrated HCl = (0.05 N) * (1 L) / (12 M) ≈ 0.0042 mL
Step 2: Dilute the Concentrated HCl
1. Wear safety goggles and gloves.
2. Label a 1-L volumetric flask with "0.05 N HCl."
3. Using a dropper or a measuring pipette, carefully add 0.0042 mL of concentrated HCl to the volumetric flask.
4. Swirl the flask gently to mix the concentrated HCl with a small amount of distilled water.
Step 3: Make up to the Mark
- Add distilled water to the 1 L mark of the volumetric flask.
- Swirl the flask gently to ensure uniform mixing of the solution.
Step 4: Check the Concentration
- Use a conductivity meter or another appropriate method to ensure the exact concentration of the prepared 0.05 N HCl solution is within an acceptable range.
-If minor adjustments are needed, you might dilute further or add more concentrated acid to reach the desired normality.
Step 5: Store Properly
- Store the prepared 0.05 N HCl solution in a labeled and sealed glass bottle.
- Store the bottle in a cool and dark place to maintain its stability.